Reagents
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Ammonium molybdate: Dissolve 15g of ammonium molybdate in 500ml of distilled water.
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Sulphuric acid: Add 140 ml of conc. H2SO4 to 900 ml distilled water.
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Ascorbic acid solution: Dissolve 27g of ascorbic acid in 500 ml distilled water.
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Potassium - Antimonyl - Tartarate (PAT): Dissolve 0.34 of PAT in 250ml of distilled water.
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Mixed reagent: To prepare 500 ml of mixed reagent, mix together 100 ml ammonium molybdate, 250ml H2SO4, 100ml ascorbic acid and 50 ml PAT. Prepare this reagent for use and discard any excess.
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Last modified: Monday, 13 February 2012, 5:47 AM